農(nóng)業(yè)部植檢所和有關(guān)研究單位與應(yīng)用單位協(xié)作進(jìn)行硫酰氟的應(yīng)用技術(shù)方面的研究結(jié)果。具體介紹硫酰氟對(duì)植物、倉儲(chǔ)害蟲、林木蛀干害蟲的毒性，對(duì)高等動(dòng)物的毒理以及中毒治療方法；硫酰氟熏蒸后的暫時(shí)殘留和永久殘留的分析測定結(jié)果；硫酰氟的常壓和真空熏蒸技術(shù)及其在農(nóng)林、植物檢疫、衛(wèi)生檢疫、外貿(mào)、文史檔案、輕紡、城建等方面大規(guī)模應(yīng)用。
浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司利用頂空氣相色譜 -電子捕獲檢測法測定玉米、大米、黃豆、大麥等糧食中熏蒸劑硫酰氟殘留量的方法。該法回收率(硫酰氟含量為2.0×10-6時(shí))為95.7%～101.3% ,相對(duì)標(biāo)準(zhǔn)偏差為1.4%～3.5% ,線性范圍在1×10-1～1×10-7 g/L ,糧食中硫酰氟檢出限低于1.0×10-8 。該法操作簡單 ,分析時(shí)間短 ,可用于糧食中殘留硫酰氟含量的檢測
名稱：毛細(xì)管柱
固定相：苯乙烯-二乙烯苯高聚物
規(guī)格： 30m*0.53mm*40um
型號(hào)：HH-PLOT Q
應(yīng)用： 食品安全國家標(biāo)準(zhǔn)植物源性食品中硫酰氟殘留量的測定氣相色譜法
The Plant Inspection Institute of the Ministry of Agriculture and relevant research units collaborated with application units to conduct research on the application technology of sulfuryl fluoride. Specifically introduce the toxicity of sulfuryl fluoride to plants, storage pests, and tree stem borers, as well as its toxicity to higher animals and treatment methods for poisoning; Analysis and determination results of temporary and permanent residues after sulfuryl fluoride fumigation; The atmospheric and vacuum fumigation technologies of sulfuryl fluoride and their large-scale applications in agriculture and forestry, plant quarantine, health quarantine, foreign trade, cultural and historical archives, light textile, urban construction, and other fields.
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. uses headspace gas chromatography electron capture detection to determine the residual amount of sulfuryl fluoride in corn, rice, soybeans, barley and other grains. The recovery rate of this method (with a sulfuryl fluoride content of 2.0 × At 10-6 hours, it ranges from 95.7% to 101.3%, with a relative standard deviation of 1.4% to 3.5%, and a linear range of 1 × 10-1～1 × 10-7 g/L, with a detection limit of less than 1.0 for sulfuryl fluoride in grains × 10-8 。 This method is simple to operate and has a short analysis time, and can be used for the detection of residual sulfuryl fluoride content in grains
Name: Capillary Column
Fixed phase: styrene divinylbenzene polymer
Specification: 30m * 0.53mm * 40um
Model: HH-PLOT Q
Application: National Food Safety Standard - Determination of Sulfuryl Fluoride Residues in Plant Derived Foods - Gas Chromatography
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